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Co-edited by world-renowned scientists in the field of catalysis, this book contains the cutting-edge in situ and operando spectroscopy characterization techniques operating under reaction conditions to determine a materials’ bulk, surface, and solution complex and their applications in the field of catalysis with emphasis on solid catalysts in powder form since such catalyst are relevant for industrial applications. The handbook covers from widely-used to cutting-edge techniques. The handbook is written for a broad audience of students and professionals who want to pursue the full capabilities available by the current state-of-the-art in characterization to fully understand how their catalysts really operate and guide the rational design of advanced catalysts.
Individuals involved in catalysis research will be interested in this handbook because it contains a catalogue of cutting-edge methods employed in characterization of catalysts. These techniques find wide use in applications such as petroleum refining, chemical manufacture, natural gas conversion, pollution control, transportation, power generation, pharmaceuticals and food processing.
Infrared (IR) Spectroscopy
Case Studies: Infrared (IR) Spectroscopy
Reflection Absorption Infrared Spectroscopy
Raman Spectroscopy
Case Studies: Raman Spectroscopy
Ultraviolet (UV) Raman Spectroscopy
Surface Enhanced Raman Spectroscopy (SERS)
Nanoscale Raman Spectroscopy
Operando Electrochemical Raman Spectroscopy
Sum Frequency Generation (SFG) Spectroscopy
Ultraviolet-Visible (UV-Vis) Spectroscopy
Case Studies: Ultraviolet-Visible (UV-Vis) Spectroscopy
Fluorescence Microscopy
Photoluminescence (PL) Spectroscopy
Case Studies: Photoluminescence (PL) Spectroscopy
Near Ambient Pressure (NAP) X-Ray Photoelectron Spectroscopy (XPS)
Case Studies: Near Ambient Pressure (NAP) X-Ray Photoelectron Spectroscopy (XPS)
Scanning Electron Microscopy (SEM)
High Pressure Transmission Electron Microscopy (TEM)
STEM High Angle Annular Dark-Field Imaging
Case Studies: Aberration Corrected High-Angle Annular Dark-Field (AC-HAADF) Microscopy
Low Energy Ion Scattering (LEIS) Spectroscopy
Case Studies: Low Energy Ion Scattering (LEIS) Spectroscopy
Neutron Scattering (NS) Spectroscopy
X-Ray Diffraction (XRD)
Case Studies: Crystallography as a Tool for Studying Methanol Conversion in Zeolites
X-Ray Absorption Spectroscopy (XAS): XANES and EXAFS
Time-Resolved X-Ray Absorption Spectroscopy (XAS)
Case Studies: Time-Resolved X-Ray Absorption Spectroscopy (XAS)
X-Ray Absorption Spectroscopy (XAS): Surface Structural Determination of Alloy Nanoparticles
Case Studies: Mapping Using X-Ray Absorption Spectroscopy (XAS) and Scattering Methods
X-Ray Microscopy and Tomography
X-Ray Absorption Spectroscopy (XAS) Combined with Other Spectroscopic Techniques
High-Field Nuclear Magnetic Resonance (NMR) Spectroscopy
Nuclear Magnetic Resonance (NMR): Modern Methods
Nuclear Magnetic Resonance (NMR): Physisorbed Xenon for Porosity
Magnetic Resonance Imaging (MRI)
Electron Paramagnetic Resonance (EPR)
Case Studies: Time-Resolved Electron Paramagnetic Resonance (EPR)
Temporal Analysis of Product (TAP)
Steady-State Isotopic Transient Kinetic Analysis (SSITKA)
Modulation Excitation Spectroscopy (MES)
Case Study 1: Modulation Excitation Spectroscopy (MES)
Case Study 2: Modulation Excitation Spectroscopy (MES)
Temperature-Programmed (TP) Techniques
Calorimetry Techniques
Case Study: Calorimetry
Chemometrics and Process Control